Product Description

1.3G/5L Rotary Evaporator w/ Chiller & Pump

A rotary
evaporator is a device used in chemical laboratories for the efficient and
gentle removal of solvents from samples by evaporation. The process of rotary
evaporation is most often used to separate solvents with low boiling points,
such a n-hexane or ethyl acetate, from compounds which are solid at room
temperature and pressure. However, careful application also allows for the
removal of a solvent from a sample containing a liquid compound, if there is
minimal co-evaporation (azeotropic behavior) and a sufficient difference in
boiling points at the chosen temperature and reduced pressure.

Example: The following table illustrates a
variety of substances, ordered by increasing vapor pressure (in absolute
units).

Ai SolventVap 1.3-gallon/5L (evaporating flask capacity)
series rotary
evaporators come with all PTFE valves for solvent-resistant
operations. Also come with them are
vertical glassware and digital temperature/rotation control. Its optimized bath
volume allows for rapid heat-up times. The condenser unit has specially
designed glass tubes that utilize surface area extremely efficiently. That’s why
our SolventVap evaporators consistently deliver reliable and reproducible
process results that are usually reserved for more costly systems. Another
important aspect of the SolventVap is the safety features, which includes
dry-run protection, water bath over-temperature shut-off protection, and fuse
protection.

Rotary evaporator features a specially designed motor and
worm gear, which provides constant rotation at speeds from 10 to 180 rpm. As
the flask containing the solvent is rotated, it continually transfers a thin
layer of liquid over the entire inner surface. This gives a very large surface
area for evaporation, which is caused by the gentle heating from the water
bath. The rotating system is fitted with a special seal that allows the
apparatus to be placed under vacuum, effectively reducing the boiling point of
the solvents and removing the vapor phase, making the process much more
efficient. Each unit is also equipped with an easy-to-use vacuum release and a
continuous feed system, which allows solvent to be constantly drawn into the
rotating flask without needing to stop the operation.

Digital water bath operates from ambient temperature to 99°C
(210°F) with PID temperature control stepping at 0.1°C increments. Heating
coils are located directly inside the pan for the most efficient heating
possible. A built-in overheat protector will shut down power, should the
controller fail.

Standard Glassware Set includes 1.32 gallon (5 liters) round-bottomed
evaporating flask, 0.79 gallon (3 liters) round-bottomed receiving flask, and
vertical condenser. Rotary evaporators with vertical glass condenser for are
great for distillation of solvents with higher boiling points.

Features

·        Solvent-resistant PTFE and Viton gaskets, ensuring long
time operation.

·        Water bath cover enhances safety by
protecting evaporating flask and the material inside; it gives you uniform
temperature inside evaporation flask as well as energy saving by reducing heat
loss. It also creates a better lab environment by preventing heat and humidity
from escaping.

·        Specialized motor with extremely compact, intermeshed
worm and worm gear provides precise driving for very quiet, vibration-free
operation.

·        Downward-condensing vacuum connection design ensures safe
vacuum operation.

·        Motorized water bath lifting for precise control.

·        Easy, straight-forward visual operation with digital
speed and temperature display.

·        PID temperature controller ensures accurate temperature
control is maintained.

·        One year warranty on rotary evaporator except glassware
and all sealing gaskets.

Your safety is important to us! Please use caution when operating. Users
of glass reaction equipment must take all necessary precautions to avoid
contact with rotating parts, particularly entanglement of loose clothing, hair,
necklaces, or other jewelry. Under these circumstances, the winding action of
the rotating parts can draw the user(s) into the apparatus, resulting in
breakage of glassware, burns, and/or chemical exposure. Extra caution must also
be taken when operating with air-reactive materials, especially under vacuum. A
leak can draw air into the apparatus and cause a violent reaction to occur.

Specifications

 Electrical requirements

 220V 50/60Hz single phase, 2300 watts
(rotation motor: 300 watts)

 Glass material

 High borosilicate glass 3.3

 Evaporating flask

 Capacity: 1.32 gallon (5 liters)
Maximum load: Not to exceed 60% of the flask's capacity
Sealing flange: 2" diameter
Rotation speed: 10 to 140 rpm
Evaporating speed: 0.5 gallon/hour (water), 1 gallon/hour
(alcohol)

 Receiving flask

 0.79 gallon (3 liter)

 Condenser

 Glassware: Dual-circulating coils,
vertical
Chilling fluid connection: 3/8" hose barb x 2
Condensing surface: 2,780 cm2 or 3 sq ft

 Working environment

 5 to 95°F

 Water bath

 Temperature range: ambient to 99°C
(210°F)
Temperature controller: digital
Dimensions: 11.4" diameter x 6.7" depth x 9" height
Material: stainless steel
Media: distilled water only
Max. water level: not to exceed 1" from the top rim of the bath
Number of heaters: one
Drain port: one
Exterior liner: rubber
Lifting: motoriezed
Maximum lifting distance: 4 inches

 Vacuum

 Level: < 3 torr
Sealing: PTFE + Viton gaskets
Connector: 3/8" hose barb x 1

 Safety

 Dry-run, over-temp shut-off, built-in
circuit breakers

 Weight & dimensions

 Shipping weight: 105 Lb (evaporator),
57 Lb (glassware)
Unit/shipping size: 30 x 15.7 x 42" / 29 x 17 x 35"
(evaporator), 22 x 22 x 22" (glassware) (WxDxH)

 Certification

 UL, CSA

Rotary Evaporator 5L

SE13-S2 Standard Package

 Part description

 Quantity

 Ai 220V C30-10 -30°C/-22°F
10L capacity recirculating chiller & fitting

1 set

 ULVAC 220V 1.6 cfm 7.5 torr
2-stage PTFE diaphragm pump & fitting

1 set

 Ai 220V SolventVap 1.3-gallon rotary
evaporator and water bath

1 set

 Vertical condenser with 2 chilling
water ports and 1 vacuum port, glass

1 pc

 1.32G/5L round shaped
rotating evaporating flask, glass

1 pc

 3L receiving flask with detachable
drain port

1 pc

 Three-way tee vapor buffering
flask, glass

1 pc

 Glass receiving flask &
condenser connector elbow with PTFE open/close switch

1 set

 Receiving flask glass vacuum
port with PTFE open/close valve

1 set

 Glass material feeding port
with PTFE open/close valve

1 set

 Glass vapor duct and vacuum
seal kit (pre-installed)

2 sets

 PTFE extension feeding hose

1 pc

 Stainless steel pole and
mechanical vacuum gauge

2 pcs

 Silicone vacuum tubing

10 ft

 Rubber-wrapped condenser and
receiving flask support and bracket

3 pcs

 Flask quick clamp (4 smaller
pcs for condenser, receiving flask and feeder, 1 larger pc for 3-way flask)
& oring

6 sets

 GL14 connector

3 pcs

 Allen key and backup inner
hex screws

4 pcs

 Ai plexiglass water bath cover for
SolventVap 5L

1 pc

 User's manual

1 pc

 

battery equipment

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