Product Description

0.5G/2L Rotary Evaporator w/ Chiller & Pump

A rotary
evaporator is a device used in chemical laboratories for the efficient and
gentle removal of solvents from samples by evaporation. The process of rotary
evaporation is most often used to separate solvents with low boiling points,
such a n-hexane or ethyl acetate, from compounds which are solid at room
temperature and pressure. However, careful application also allows for the
removal of a solvent from a sample containing a liquid compound, if there is
minimal co-evaporation (azeotropic behavior) and a sufficient difference in
boiling points at the chosen temperature and reduced pressure.

 

Example: The following table is a list of a
variety of substances ordered by increasing vapor pressure (in absolute units).

The
new Ai SolventVap 0.5-gallon/2L (evaporating flask
capacity) series rotary evaporators come with a modular heating
bath, vertical glassware, and digital temperature/rotation control. Its
optimized bath volume allows for rapid heat-up times. The condenser unit has
specially designed glass tubes that utilize surface area extremely efficiently.
That’s why our SolventVap evaporators consistently deliver reliable and
reproducible process results that are usually reserved for more costly systems.
Another important aspect of the SolventVap is the safety features, which
includes dry-run protection, water bath over-temperature shut-off protection,
and fuse protection.

Rotary evaporator features a specially designed motor and
worm gear, which provides constant rotation at speeds from 10 to 180 rpm. As
the flask containing the solvent is rotated, it continually transfers a thin
layer of liquid over the entire inner surface. This gives a very large surface
area for evaporation, which is caused by the gentle heating from the water
bath. The rotating system is fitted with a special seal that allows the
apparatus to be placed under vacuum, effectively reducing the boiling point of
the solvents and removing the vapor phase, making the process much more
efficient. Each unit is also equipped with an easy-to-use vacuum release and a
continuous feed system, which allows solvent to be constantly drawn into the
rotating flask without needing to stop the operation.

Digital water bath operates from ambient temperature to 99°C
(210°F) with PID temperature control stepping at 0.1°C increments. Heating
coils are located directly inside the pan for the most efficient heating
possible. A built-in overheat protector will shut down power, should the
controller fail.

Standard Glassware Set 0.13 gallon (0.5L), 0.26 gallon (1L) or 0.53
gallon (2 liters) pear shaped evaporating flask, 0.26 gallon (1 liter)
round-bottomed receiving flask, and vertical condenser. Rotary evaporators
with vertical glass condenser are great for distillation of solvents with
higher boiling points.

Features

·        Solvent-resistant PTFE and Viton gaskets ensuring long
time operation.

·        Specialized motor with extremely compact, intermeshed
worm and worm gear provides precise driving for very quiet, vibration-free
operation.

·        Downward-condensing vacuum connection design ensures safe
vacuum operation.

·        Modular design (individual rotary and water bath modules)
for easy future upgrades.

·        Easy multi-level manual lift with secure lock for the
evaporating flask.

·        Easy, straight-forward visual operation with digital
speed and temperature display.

·        PID temperature controller ensures accurate temperature
control is maintained.

Your safety is important to us! Please use caution when
operating. Users of glass reaction equipment must take all necessary
precautions to avoid contact with rotating parts, particularly entanglement of
loose clothing, hair, necklaces, or other jewelry. Under these circumstances,
the winding action of the rotating parts can draw the user(s) into the
apparatus, resulting in breakage of glassware, burns, and/or chemical exposure.
Extra caution must also be taken when operating with air-reactive materials,
especially under vacuum. A leak can draw air into the apparatus and cause a
violent reaction to occur.

Specifications

 Electrical requirements

 110V 60Hz single phase, 9.8A, 1075
watts (heater: 1050 watts, rotation motor: 25 watts)

 Glass material

 High borosilicate glass 3.3

 Evaporating flask

 Capacity: 0.13 gallon (0.5L), 0.26
gallon (1L) or 0.53 gallon (2L)
Maximum load: Not to exceed 60% of the flask's capacity
Rotation speed: 10 to 180 rpm
Evaporating speed: 20 ml per minute
Lifting: weight balancing manual control with lock
Max lifting distance: 4 inches (extendable to 10 inches)

 Receiving flask

 0.26 gallon (1L)

 Condenser

 Glassware: Vertical with dual-spiral
glass tubing
Chilling fluid connection: 3/8" hose barb x 2
Vacuum connection: 3/8" hose barb x 1
Condensing surface: 1,260 cm2 or 1.4 sq ft

 Working environment

 5 to 95°F

 Water bath

 Max. temp: 99°C (210°F)
Temp controller: digital
Capacity: 2 gallons
Material: stainless steel
Dimensions: 10" diameter x 5" depth x 9.75" height
Media: distilled water only
Max. water level: not to exceed 1" from the top rim of the bath
Number of heaters: one

 Vacuum

 Connection: 3/8" hose barb x 1
(on condenser)
Sealing: PTFE + Viton gaskets
Ultimate vacuum: < 3 torrs

 Safety

 Dry-run, over-temp shut-off, fuse
protections

 Weight & dimensions

 Rotary evaporator unit/shipping: 21 /
40 Lb
Rotary evaporator unit/shipping: 22 x 12.5 x 26" / 26 x 21 x
29" (WxDxH)

 Warranty

 One year warranty on rotary
evaporator except glassware and all sealing gaskets.
Glassware may have minute blemishes that will not affect the function.
If you believe there are imperfections on your glassware, please
contact us.
We check all our inventory and make sure no defective glassware is sent
to our customers.

Chiller & Pump Evaporator

SE05-S1 Standard Package

 Part description

 Qty

 Ai 110V C15-3 -15°C/5°F compact
recirculating chiller and accessories

1 set

 Ai 110V WaterVac 0.7 cfm 735 torr
2-head recirculating water pump

1 pc

 Premium food grade silicone vacuum
hose

6 ft

 110V evaporator body

1 pc

 110V water bath

1 pc

 Vertical condenser with 2
chilling water ports and 1 vacuum port, glass

1 pc

 2L pear shaped evaporating
flask, glass
(choose based on volume of material to load)

1 pc

 0.26G/1L round shaped
receiving flask, glass

1 pc

 Glass vapor duct with seal

1 set

 Glass material feeding tube
with valve & PTFE extension hose

1 pc

 PTFE vacuum sealing kit

1 set

 Condenser cap kit

2 pcs

 Glass shaft cap and
evaporator flask quick-release

2 pcs

 Condenser support and bracket

1 pc

 Condenser support securing
screw

1 pc

 Receiving flask ball joint
clamp

1 pc

 GL14 connector

3 pcs

 3-prong 110V US power cord
for evaporator

1 pc

 Silicone vacuum tubing

10 ft

 Mechanical vacuum gauge

1 pc

 User's manual

2 pcs

battery equipment

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